Overview
ABSTRACT
Although the scratch test has now become commonplace both in research as a measurement tool and in industry as a Quality Control method, its utility in gaining a quantitative measure of the adhesion of a coating has only been approached in the past few years. This article provides a timely review of recent progress made in extracting quantitative data from the scratch test. The combined use of the scratch test with other techniques has revealed additional data on sub-surface events that were not previously accessible. This article reviews these developments and looks ahead at future challenges.
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Read the articleAUTHORS
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Guillaume BERTHOUT: Product Manager - Anton Paar France, Courtaboeuf, France
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Nicholas X. RANDALL: Lead Scientist and Product Manager - Anton Paar TriTec, Peseux, Switzerland
INTRODUCTION
This article provides a detailed analysis of instrumented scratch testing techniques. These devices are generally used to qualitatively characterize coatings and thin films. Interpretation of the data delivered by these instruments has been facilitated by the advent of high-performance tools such as panoramic imaging, scratch test profile tracking and spatial synchronization during optical observation of a scratch. In addition, the ability to model the deformation of a coating and its substrate as a function of applied load means that test parameters can be adjusted to favor positioning of the maximum stress field not far from the interface. This has led to the development of a wide range of indenters with appropriate contact conditions and pressures.
Significant progress has also been made in using the scratch technique to measure mechanical properties related to adhesion, such as toughness, hardness and viscoelasticity. Similarly, the combined use of scratch testing with other techniques such as acoustic microscopy, Raman spectroscopy, in situ microscopy, etc. has provided additional information on induced damage (cracking, fatigue, fracture) that was not previously systematically accessible or exploitable. The article reviews these developments and outlines the challenges ahead.
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KEYWORDS
coatings adherence | scratch resistance | sub-surface damages | extracting data
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Friction, wear and lubrication
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Scratch tests
Bibliography
Websites
Anton Paar Scratch Testers
http://www.anton-paar.com/corp-en/products/group/scratch-tester/
Standards and norms
- Standard test method for evaluating adhesion by knife, ASTM International - ASTM D6677 -
- Standard test methods for rating adhesion by tape test, ASTM International - ASTM D3359 -
- Standard test method for film hardness by pencil test, ASTM International - ASTM D3363 -
- Standard test method for pull-off strength of coatings using portable adhesion testers, ASTM International - ASTM D4541 - ...
Patents
European Patent EP2065695 Method for analyzing a scratch test (2009)
European Patent EP1092142 Test apparatus and method of measuring mar resistance of film or coaking
European Patent EP16178524.1 Methods for surface evaluation
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