Overview
ABSTRACT
Knowing and quantifying microstructures before and after thermal, thermochemical or thermomechanical treatments is essential to mastering the properties of metal alloys.
This article describes the possibilities for surface and volume quantification of microstructures, and the specific issues involved. It details current norms and practices, as well as the most recent techniques for quantitative metallography in two and three dimensions, such as X-ray micro-tomography and layer micro-tomography, as well as mathematical approaches such as the Saltykov method.
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Read the articleAUTHOR
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Thomas MUNCH: ENSAIS engineer - Agrégé en Mécanique, Saint-Louis, France
INTRODUCTION
Generally speaking, the transformation of metal alloys by wrought, thermal and thermochemical treatments determines their properties of use. Knowing and quantifying microstructures before and after thermal, thermochemical or thermomechanical treatments is essential for controlling their effects and managing the process.
These processes are based on two types of data, the most common measurement methods of which are :
analysis of physico-chemical transformation points (thermal, dilatometric and magnetic analysis), which is the subject of article
;[M 90] analysis of microstructures (or constituent topography: quantity, shape, phase dispersion) by optical or electron microscopy and associated techniques, which is the subject of the article
.[M 91]
This article describes the possibilities of surface and volume quantification of microstructures, specific problems and standardized solutions. The application of these techniques provides the metallographic knowledge needed to optimize the choice of materials and their processing, which is crucial for maximizing the efficiency of the product-process-material triptych, and ultimately the suitability of the product, from both a technical-economic and environmental point of view.
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KEYWORDS
quantification | Metallography | microstructures | micro-tomography | Saltykov
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Studies and properties of metals
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Quantitative metallography
Bibliography
Standards and norms
- Steels – Micrographic determination of apparent grain size - NF EN ISO 643 - 2020
- Test Methods for Determining Average Grain Size - ASTM E112-24 - 2024
- Steels – Metallographic characterization of duplex grain size and distribution - ISO 14250 - 2000
- Steels – Determining the content of non-metallic inclusions – Micrographic method using standard images - ISO 4967 - 2013
- Steel products –...
Directory
Manufacturers – Suppliers – Distributors (non-exhaustive list)
Leica Microsystems: microscopy https://www.leica-microsystems.com/fr/
Olympus: microscopy https://www.evidentscientific.com/fr/
Zeiss: microscopy...
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