Article | REF: M4127 V1

Electron diffraction: parallel illumination

Authors: Richard A. PORTIER, Philippe VERMAUT, Bernard JOUFFREY

Publication date: March 10, 2008

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ABSTRACT

Matter can be explored at the atomic scale due to the interaction between atoms and an incident radiation of a wavelength comparable or inferior to interatomic distances. Thus, the diffraction of the electrons obtained in practice with an electron microscope provides extremely rich information on crystal. This technique makes high-energy electrons interact with the crystalline potential of a thin specimen. After having briefly described an electron microscope, this article presents the current techniques used for these rapid matter electron interactions. One of their major interest is the very local nature of the information. Indeed, it is possible to obtain sizes of probes of the order of the nanometer.

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AUTHORS

  • Richard A. PORTIER: Structural Metallurgy Group (UMR CNRS 7045) - École nationale supérieure de chimie de Paris

  • Philippe VERMAUT: Structural Metallurgy Group (UMR CNRS 7045) - École nationale supérieure de chimie de Paris

  • Bernard JOUFFREY: MSS-Mat Laboratory (UMR CNRS 8579) - École Centrale de Paris

 INTRODUCTION

After detailing the characteristics of radiation-matter interaction and highlighting the differences between electron radiation, X-rays and neutrons in the [M 4 125] and [M 4 126] files, we will now turn our attention to electron diffraction obtained in practice with an electron microscope. These are high-energy electrons that interact strongly with the crystalline potential of a thin specimen in different experimental situations, thanks to the great flexibility of illumination conditions obtainable with a modern microscope.

Starting with a brief description of the basic principle of an electron microscope, we'll see how the conditions for diffraction at infinity (Fraunhoffer diffraction [M 4 126] ) are achieved. It will therefore be highly instructive to examine the "geometric" correspondence between a known two-dimensional object and its diffraction pattern obtained by Fourier transformation. Next, we'll look at the different ways of acquiring information in reciprocal space [M 4 125] , after briefly pointing out the fundamental consequence of fast electron diffraction.

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Electron diffraction: parallel illumination