Overview
ABSTRACT
This article presents a comparative study of three approaches of measurements uncertainties evaluation: GUM, GUM S1 and global. This work will enable us to take advantage of the complementarity of the three approaches, for a better understanding of the measurement process and to be able to control it and improve it if necessary. To compare these approaches, we calibrated a pH meter with pH solutions calibrated within an accredited laboratory, to evaluate uncertainties using the same measurement results.
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Read the articleAUTHORS
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Abdelali MOHAMMADI: Doctoral student - Cadi Ayyad University, Marrakech, Morocco
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Youssef EL HACHIMI: Professor-researcher - Cadi Ayyad University, Marrakech, Morocco
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Samira MARICHANE: Metrology manager - Office national de Sécurité Sanitaire des produits Alimentaires – Laboratoire régional d'Analyses et de Recherches de Marrakech, Morocco
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Abdallah MOUAD: Quality Manager - Office national de Sécurité Sanitaire des produits Alimentaires – Laboratoire régional d'Analyses et de Recherches de Marrakech, Morocco
INTRODUCTION
One of the missions of the Office National de Sécurité Sanitaire des Produits Alimentaires (ONSSA) is to protect consumers. In this context, the reliability of food product control is crucial.
Various analyses carried out by the ONSSA laboratory allow us to assess the conformity of food products to current standards.
The performance of an analysis relies to a large extent on equipment, made up of: (i) measuring equipment, i.e. the device used to take a measurement and give the value of a quantity, (ii) analysis equipment, which provides a result, and (iii) intermediate equipment, which takes part in obtaining it.
Generally speaking, metrology is used to monitor the measurement process and ensure that measuring instruments are working properly. It ensures that measurements are taken to enable tests to be carried out in compliance with standards and requirements.
In order to optimize the interpretation of measurement results, it is essential to control the uncertainties associated with them. Several approaches can be used to estimate these uncertainties.
This is the background to the work carried out by the metrology and quality section of the Marrakech Regional Laboratory for Analysis and Research. This department is committed to continuous improvement, and is part of a quality management system drawn up by ONSSA.
This article presents a comparative study of the most widely used approaches to uncertainty assessment: GUM (Guide to the Expression of Uncertainty in Measurement), GUM S1 (Supplement 1 to GUM) and global, and how to take advantage of the complementarity of these approaches to meet measurement quality and reliability requirements.
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KEYWORDS
uncertainty | calibration | pH meter | GUM | Monte Carlo | Global
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Instrumentation and measurement methods
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Comparative study of three uncertainty assessment approaches: GUM, GUM S1 and global
Bibliography
Websites
VIM 3: international vocabulary of metrology, Bureau International des Poids et Mesures (BIPM) website: https://www.bipm.org/fr/publications/guides/vim.html (page consulted on February 8, 2019)
Standards and norms
AFNOR
- Metrology – Monte Carlo evaluation of measurement uncertainty – Principles and implementation of GUM Supplement 1. AFNOR - FD X07-023 - 2012
- Exactitude (justesse et fidélité) des résultats et méthodes de mesure. Partie 2 : Méthode de base pour la détermination de la répétabilité et de la reproductibilité d'une méthode de mesure normalisée. IMANOR - NM...
IMANOR
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