Article | REF: J8015 V1

Benchtop NMR spectrometers for the in-line monitoring of continuous flow reactions

Authors: Patrick GIRAUDEAU, François-Xavier FELPIN

Publication date: May 10, 2019

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3. Reaction monitoring by 1H BC NMR

Integrating an on-line analysis system into a flow reactor eliminates the problem of availability of analysis equipment, which is often located outside the synthesis laboratory and shared by several research projects. In addition, on-line analysis offers the advantage of obtaining essential information on the nature of the reaction medium without special handling, particularly when the reaction mixture contains unstable and/or toxic compounds. Legros et al. have taken advantage of the benefits of on-line NMR analysis to propose a portable device for the destruction of mustards in flow.

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Reaction monitoring by 1H BC NMR