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6. Using BC NMR in self-contained flow reactors
On-line monitoring of flow reactions using NMR spectrometers makes
it possible to modify or adjust experimental conditions very quickly,
to maximize or minimize an objective (yield, productivity, cost, etc.),
since a simple
1
H analysis can provide information on the
content of a reaction crude in just a few tens of seconds. In this
context, a new generation of autonomous flow reactors has emerged
in recent years. To date, only a handful of teams worldwide have mastered
these autonomous technologies, which require knowledge at the frontier
of computer programming, chemical engineering and organic synthesis.
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Using BC NMR in self-contained flow reactors
Bibliography
Directory
Benchtop NMR spectrometers from the following suppliers:
Magritek
Nanalysis
Oxford Instruments
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