1. Description of a purification cabinet
1.1 Requirements
The chambers in which noble gas purification takes place are designed to reduce the sources of external contamination (degassing, permeation, backscattering, etc.) that can affect the accuracy of isotope ratio measurements and/or elemental fractionation analysis. In fact, there are many species, most often organic, which interfere with noble gases in a non-resolved way during mass spectrometry measurements, and whose impact must be minimized. It is therefore advisable to design purification chambers entirely in stainless steel, as this material has the advantage of being non-porous, even with helium, and of offering extremely low outgassing rates, compatible with ultra-high vacuum. The enclosure, initially at atmospheric pressure during assembly, must be designed to...
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Description of a purification cabinet
Bibliography
Events
DINGUE (Development In Noble Gas Understanding and Expertise ). Workshop organized each year in conjunction with the GOLDSCHIMDT conference.
Standards and norms
- CF flange connection elements: The elements are made of 316L stainless steel [(DIN 17 440) – WN 14 404) Z2CND 17-12]. - « Pneurop » 6601/1981 et DIN 28 403 -
- Cuivre OFHC (Oxygen Free High Conductivity) : Cuivre élaboré suivant une méthode américaine. Son équivalent français est le cuivre Cu-c1 ou 2. - ISO 431 -
- Méthode gravamétrique de préparation des mélanges gazeux dans une bouteille à des fins d'étalonnage...
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